Computed Properties of C8H11NO. Jia, JH; Wei, HQ; Duan, YQ; Ning, HX; Yu, J; Zhu, Y; Hou, WB; Li, YL in [Jia, Jianhua; Wei, Huiqiang; Duan, Yuqing; Ning, Hongxin; Yu, Jiang; Zhu, Yuan; Hou, Wenbin; Li, Yiliang] Peking Union Med Coll, Inst Radiat Med, Tianjin Key Lab Radiat Med & Mol Nucl Med, Tianjin 300192, Peoples R China; [Jia, Jianhua; Wei, Huiqiang; Duan, Yuqing; Ning, Hongxin; Yu, Jiang; Zhu, Yuan; Hou, Wenbin; Li, Yiliang] Chinese Acad Med Sci, Tianjin 300192, Peoples R China; [Jia, Jianhua; Li, Yiliang] Tianjin Univ Tradit Chinese Med, Tianjin 301617, Peoples R China published An Improved Synthesis of the Triethylene Glycol-Substituted 4-(N-Methyl-N-Boc-Amino)Styrylpyridine in 2020.0, Cited 11.0. The Name is 2-(4-Aminophenyl)ethanol. Through research, I have a further understanding and discovery of 104-10-9.
An improved five-step synthesis of triethylene glycol-substituted 4-(N-methyl-N-Boc-amino)styrylpyridine (6) is described. Using cost-effective starting materials, the developed synthesis route was synthetic, efficient, and chromatographic purification-free. The key point of the work is the one-pot synthesis of tert-butyl methyl(4-vinylphenyl)carbamate through methylation and elimination in the NaH/THF system. The new synthesis route shows the potential to achieve scaled-up preparation of 6 in the future.
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Reference:
Amide – Wikipedia,
,Amide – an overview | ScienceDirect Topics